TA Instruments

AR1710-0001f

04/09/2012 16:58:31

Sample name	ASW 10 mm from base, 60 mm to top, disk 9 PMMA fouled
Sample notes	 
Experiment notes	Plastic parallel plate with adaptor supplied by Southampton Uni., on ETC rod with grub screws.

Distances fromlower surface of PP plate. Southampton container.
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1710
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	04/09/2012 16:58:31

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	22.4 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:01:00 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:00:30 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	22.4 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	3.100 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.262 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	3
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	18.42 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

-12.73	7.651	-1.664	1.0000	22.4	443.9	5.3941	10000	0.1090	7.584	6.7426	674.26	3.383E-3	0.0	1.0	61.000	-39.052	6.120
0.8794	12.29	0.07158	1.9960	22.4	444.7	13.3456	10000	0.1092	2.946	16.682	1668.2	3.383E-3	0.0	1.0	61.996	2.6981	9.829
1.623	19.33	0.08393	3.0120	22.4	445.6	26.8419	10000	0.1094	1.192	33.552	3355.2	3.383E-3	0.1	1.1	63.012	4.9780	15.47
2.231	23.02	0.09692	3.9960	22.4	448.0	40.7859	10000	0.1100	0.8457	50.982	5098.2	3.383E-3	0.1	1.1	63.996	6.8437	18.41
3.575	30.84	0.1159	5.0120	22.4	438.1	68.0390	10000	0.1075	0.4607	85.049	8504.9	3.383E-3	0.1	1.1	65.012	10.969	24.67
5.510	39.46	0.1396	6.0000	22.4	432.3	106.5700	10000	0.1061	0.2776	133.21	13321	3.383E-3	0.1	1.1	66.000	16.905	31.57
6.287	42.52	0.1479	6.9960	22.4	447.2	126.1870	10000	0.1098	0.2474	157.73	15773	3.384E-3	0.1	1.1	66.996	19.290	34.01
7.999	49.12	0.1629	8.0120	22.4	439.0	165.1590	10000	0.1077	0.1820	206.45	20645	3.384E-3	0.1	1.1	68.012	24.540	39.29
10.53	57.53	0.1830	8.9960	22.4	426.6	223.0600	10000	0.1047	0.1289	278.83	27883	3.384E-3	0.1	1.1	68.996	32.296	46.02
12.60	63.68	0.1979	10.004	22.4	419.9	274.6280	10000	0.1031	0.1035	343.29	34329	3.384E-3	0.2	1.2	70.004	38.669	50.95
14.37	69.64	0.2063	10.996	22.4	418.3	326.0030	10000	0.1027	0.08624	407.50	40750	3.384E-3	0.2	1.2	70.996	44.077	55.72
16.25	75.11	0.2163	12.012	22.4	421.6	377.4020	10000	0.1035	0.07472	471.75	47175	3.384E-3	0.2	1.2	72.012	49.844	60.09
18.22	80.51	0.2263	12.996	22.4	415.8	434.6650	10000	0.1021	0.06415	543.33	54333	3.383E-3	0.2	1.2	72.996	55.903	64.41
20.78	86.43	0.2405	13.996	22.4	413.3	499.0770	10000	0.1014	0.05533	623.85	62385	3.384E-3	0.2	1.2	73.996	63.761	69.14
24.05	94.60	0.2543	15.000	22.4	424.9	594.0890	10000	0.1043	0.04748	742.61	74261	3.384E-3	0.3	1.3	75.000	73.798	75.68
26.30	99.91	0.2633	16.012	22.4	425.7	664.1950	10000	0.1045	0.04265	830.24	83024	3.383E-3	0.3	1.3	76.012	80.693	79.93
28.45	105.7	0.2693	16.996	22.4	411.7	740.5690	10000	0.1010	0.03688	925.71	92571	3.383E-3	0.3	1.3	76.996	87.283	84.53
32.00	113.7	0.2814	17.996	22.4	399.3	855.3580	10000	0.09800	0.03087	1069.2	1.0692E5	3.383E-3	0.3	1.3	77.996	98.179	90.98
34.76	118.8	0.2927	18.996	22.4	408.4	931.1140	10000	0.1002	0.02894	1163.9	1.1639E5	3.383E-3	0.3	1.3	78.996	106.66	95.03
37.33	124.2	0.3004	19.992	22.4	384.4	1020.1400	10000	0.09434	0.02490	1275.2	1.2752E5	3.383E-3	0.3	1.3	79.992	114.52	99.39
41.01	132.3	0.3101	21.020	22.4	389.4	1154.6899	10000	0.09556	0.02225	1443.4	1.4434E5	3.383E-3	0.4	1.4	81.020	125.83	105.8
44.12	137.4	0.3212	21.992	22.4	388.5	1241.9900	10000	0.09536	0.02059	1552.5	1.5525E5	3.384E-3	0.4	1.4	81.992	135.35	109.9
46.64	142.8	0.3266	22.996	22.4	385.2	1343.4200	10000	0.09455	0.01889	1679.3	1.6793E5	3.384E-3	0.4	1.4	82.996	143.10	114.2
50.93	150.8	0.3377	24.000	22.4	383.6	1495.4399	10000	0.09414	0.01687	1869.3	1.8693E5	3.384E-3	0.4	1.4	84.000	156.24	120.6
53.88	155.9	0.3456	25.020	22.4	394.3	1596.7600	10000	0.09678	0.01622	1996.0	1.9960E5	3.384E-3	0.4	1.4	85.020	165.31	124.7
57.42	161.3	0.3560	26.000	22.4	385.2	1711.9100	10000	0.09455	0.01480	2139.9	2.1399E5	3.384E-3	0.4	1.4	86.000	176.17	129.1
60.89	169.3	0.3596	27.004	22.4	371.2	1882.8700	10000	0.09110	0.01295	2353.6	2.3536E5	3.384E-3	0.5	1.5	87.004	186.81	135.4
63.86	174.4	0.3661	28.012	22.4	361.2	1995.5601	10000	0.08866	0.01187	2494.5	2.4945E5	3.383E-3	0.5	1.5	88.012	195.91	139.5
67.73	179.5	0.3772	29.012	22.4	368.7	2115.8301	10000	0.09049	0.01144	2644.8	2.6448E5	3.383E-3	0.5	1.5	89.012	207.78	143.6
72.58	187.5	0.3870	30.016	22.4	364.6	2307.2000	10000	0.08947	0.01037	2884.0	2.8840E5	3.384E-3	0.5	1.5	90.016	222.66	150.0
75.38	192.7	0.3912	31.008	22.4	343.9	2432.0701	10000	0.08440	9.262E-3	3040.1	3.0401E5	3.384E-3	0.5	1.5	91.008	231.26	154.1
79.35	197.8	0.4011	31.996	22.4	366.2	2565.6101	10000	0.08988	9.358E-3	3207.0	3.2070E5	3.384E-3	0.5	1.5	91.996	243.44	158.3
83.99	205.8	0.4081	33.016	22.4	357.9	2773.3999	10000	0.08785	8.450E-3	3466.8	3.4668E5	3.384E-3	0.6	1.6	93.016	257.68	164.6
88.06	211.0	0.4174	34.012	22.4	338.9	2913.1399	10000	0.08319	7.615E-3	3641.4	3.6414E5	3.384E-3	0.6	1.6	94.012	270.15	168.8
93.78	218.6	0.4290	35.004	22.4	340.6	3131.7800	10000	0.08359	7.128E-3	3914.7	3.9147E5	3.384E-3	0.6	1.6	95.004	287.70	174.9
97.21	223.9	0.4342	36.012	22.4	319.9	3280.2400	10000	0.07852	6.382E-3	4100.3	4.1003E5	3.384E-3	0.6	1.6	96.012	298.24	179.1
100.8	229.1	0.4399	37.012	22.4	335.6	3507.0100	10000	0.08237	6.396E-3	4383.8	4.3838E5	3.384E-3	0.6	1.6	97.012	309.17	183.3
106.0	236.6	0.4478	38.016	22.4	314.1	3657.8201	10000	0.07710	5.611E-3	4572.3	4.5723E5	3.383E-3	0.6	1.6	98.016	325.11	189.3
109.4	241.8	0.4525	39.000	22.4	324.9	3821.9600	10000	0.07974	5.555E-3	4777.5	4.7775E5	3.383E-3	0.7	1.7	99.000	335.71	193.5
115.9	249.6	0.4642	40.008	22.4	326.5	4069.2600	10000	0.08014	5.242E-3	5086.6	5.0866E5	3.384E-3	0.7	1.7	100.008	355.44	199.7
120.1	254.6	0.4718	40.996	22.4	305.9	4233.5698	10000	0.07507	4.718E-3	5292.0	5.2920E5	3.384E-3	0.7	1.7	100.996	368.55	203.7
126.7	262.4	0.4827	42.016	22.4	291.0	4499.9399	10000	0.07142	4.225E-3	5624.9	5.6249E5	3.384E-3	0.7	1.7	102.016	388.65	210.0
129.2	267.6	0.4827	43.012	22.4	299.2	4674.1401	10000	0.07345	4.179E-3	5842.7	5.8427E5	3.383E-3	0.7	1.7	103.012	396.28	214.1
133.8	272.7	0.4906	44.012	22.4	291.8	4850.9702	10000	0.07162	3.925E-3	6063.7	6.0637E5	3.383E-3	0.7	1.7	104.012	410.44	218.1
140.8	280.4	0.5021	45.012	22.4	286.8	5128.6602	10000	0.07040	3.650E-3	6410.8	6.4108E5	3.384E-3	0.8	1.8	105.012	431.83	224.3
143.7	285.5	0.5034	46.012	22.4	265.4	5317.9800	10000	0.06513	3.256E-3	6647.5	6.6475E5	3.384E-3	0.8	1.8	106.012	440.89	228.4
151.7	293.1	0.5176	47.016	22.4	271.1	5603.0000	10000	0.06655	3.156E-3	7003.8	7.0038E5	3.384E-3	0.8	1.8	107.016	465.39	234.5
154.4	298.1	0.5178	48.012	22.4	260.4	5797.4800	10000	0.06391	2.930E-3	7246.9	7.2469E5	3.384E-3	0.8	1.8	108.012	473.66	238.5
158.0	303.3	0.5208	49.012	22.4	266.2	5999.2798	10000	0.06533	2.893E-3	7499.1	7.4991E5	3.384E-3	0.8	1.8	109.012	484.67	242.7
166.3	310.9	0.5350	50.048	22.4	251.3	6301.9702	10000	0.06168	2.599E-3	7877.5	7.8775E5	3.384E-3	0.8	1.8	110.048	510.34	248.8
170.1	316.0	0.5382	51.000	22.4	267.0	6510.2300	10000	0.06553	2.674E-3	8137.8	8.1378E5	3.383E-3	0.9	1.9	111.000	521.81	252.8
176.5	323.8	0.5450	51.996	22.4	243.9	6834.0698	10000	0.05985	2.326E-3	8542.6	8.5426E5	3.384E-3	0.9	1.9	111.996	541.39	259.0
181.6	328.9	0.5521	52.996	22.4	242.2	7046.1899	10000	0.05945	2.239E-3	8807.7	8.8077E5	3.383E-3	0.9	1.9	112.996	557.01	263.1
186.4	336.4	0.5540	54.016	22.4	249.6	7375.7300	10000	0.06127	2.206E-3	9219.7	9.2197E5	3.384E-3	0.9	1.9	114.016	571.82	269.1
191.6	341.6	0.5609	55.000	22.4	251.3	7603.4102	10000	0.06168	2.154E-3	9504.3	9.5043E5	3.383E-3	0.9	1.9	115.000	587.78	273.3
200.3	346.7	0.5779	56.000	22.4	195.1	7828.2002	10000	0.04788	1.623E-3	9785.3	9.7853E5	3.383E-3	0.9	1.9	116.000	614.63	277.4
205.2	354.2	0.5792	57.012	22.4	210.8	8168.6499	10000	0.05174	1.680E-3	10211	1.0211E6	3.384E-3	1.0	2.0	117.012	629.43	283.4
209.3	359.3	0.5825	57.996	22.4	228.2	8408.2002	10000	0.05600	1.767E-3	10510	1.0510E6	3.384E-3	1.0	2.0	117.996	642.18	287.5
217.5	367.0	0.5928	59.012	22.4	193.4	8767.5303	10000	0.04748	1.436E-3	10959	1.0959E6	3.384E-3	1.0	2.0	119.012	667.41	293.6
223.5	372.0	0.6007	60.016	22.4	200.9	9007.1299	10000	0.04930	1.452E-3	11259	1.1259E6	3.383E-3	1.0	2.0	120.016	685.57	297.6

Peak hold step

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

226.1	375.0	0.6029	0.99200	22.4	191.0	293.2440	10000	0.04687	1.358E-3	366.56	36656	3.384E-3	0.0	2.0	121.992	693.65	300.0
226.6	375.0	0.6044	1.9920	22.4	161.2	549.4230	10000	0.03956	1.146E-3	686.78	68678	3.384E-3	0.0	2.0	122.992	695.34	300.0
224.8	375.0	0.5995	2.9920	22.4	231.5	923.9580	10000	0.05681	1.646E-3	1154.9	1.1549E5	3.383E-3	0.0	2.1	123.992	689.75	300.0
225.4	375.0	0.6009	3.9960	22.4	225.7	1173.1400	10000	0.05539	1.605E-3	1466.4	1.4664E5	3.383E-3	0.1	2.1	124.996	691.37	300.0
229.7	375.0	0.6126	4.9920	22.4	187.6	1424.4600	10000	0.04606	1.334E-3	1780.6	1.7806E5	3.383E-3	0.1	2.1	125.992	704.77	300.0
223.7	375.0	0.5965	5.9960	22.4	197.6	1802.9900	10000	0.04849	1.405E-3	2253.7	2.2537E5	3.384E-3	0.1	2.1	126.996	686.30	300.0
228.2	375.0	0.6086	6.9920	22.4	188.5	2052.6299	10000	0.04626	1.340E-3	2565.8	2.5658E5	3.384E-3	0.1	2.1	127.992	700.18	300.0
226.3	375.0	0.6034	7.9920	22.4	197.6	2306.7600	10000	0.04849	1.405E-3	2883.5	2.8835E5	3.384E-3	0.1	2.1	128.992	694.19	300.0
227.2	375.0	0.6057	9.0000	22.4	172.8	2682.7900	10000	0.04240	1.229E-3	3353.5	3.3535E5	3.384E-3	0.2	2.2	130.000	696.91	300.0
226.2	375.0	0.6033	9.9920	22.4	184.3	2936.2900	10000	0.04524	1.311E-3	3670.4	3.6704E5	3.384E-3	0.2	2.2	130.992	694.05	300.0
228.3	375.0	0.6088	11.000	22.4	201.7	3309.3401	10000	0.04951	1.434E-3	4136.7	4.1367E5	3.384E-3	0.2	2.2	132.000	700.43	300.0
227.7	375.0	0.6073	11.992	22.4	167.8	3560.6899	10000	0.04119	1.193E-3	4450.9	4.4509E5	3.384E-3	0.2	2.2	132.992	698.70	300.0
225.7	375.0	0.6018	13.056	22.4	186.8	3938.8999	10000	0.04585	1.328E-3	4923.6	4.9236E5	3.383E-3	0.2	2.2	134.056	692.40	300.0
226.9	375.0	0.6050	13.992	22.4	189.3	4188.9800	10000	0.04646	1.346E-3	5236.2	5.2362E5	3.383E-3	0.2	2.2	134.992	696.03	300.0
221.1	375.0	0.5896	15.024	22.4	259.6	4440.2300	10000	0.06371	1.846E-3	5550.3	5.5503E5	3.383E-3	0.3	2.3	136.024	678.41	300.0
223.4	375.0	0.5957	15.992	22.4	248.0	4818.5801	10000	0.06087	1.764E-3	6023.2	6.0232E5	3.383E-3	0.3	2.3	136.992	685.33	300.0
223.0	375.0	0.5947	16.992	22.4	216.6	5068.6802	10000	0.05316	1.540E-3	6335.9	6.3359E5	3.383E-3	0.3	2.3	137.992	684.24	300.0
226.8	375.0	0.6049	17.992	22.4	181.0	5319.9502	10000	0.04443	1.287E-3	6649.9	6.6499E5	3.383E-3	0.3	2.3	138.992	695.90	300.0
223.7	375.0	0.5965	19.004	22.4	157.1	5696.8101	10000	0.03855	1.117E-3	7121.0	7.1210E5	3.384E-3	0.3	2.3	140.004	686.25	300.0
224.9	375.0	0.5997	19.992	22.4	169.5	5948.3301	10000	0.04159	1.205E-3	7435.4	7.4354E5	3.383E-3	0.3	2.3	140.992	689.98	300.0
227.7	375.0	0.6072	20.992	22.4	169.5	6217.5698	10000	0.04159	1.205E-3	7772.0	7.7720E5	3.383E-3	0.3	2.4	141.992	698.50	300.0
225.6	375.0	0.6017	21.992	22.4	201.7	6576.5698	10000	0.04951	1.434E-3	8220.7	8.2207E5	3.384E-3	0.4	2.4	142.992	692.28	300.0
225.2	375.0	0.6004	22.992	22.4	182.7	6829.6099	10000	0.04484	1.299E-3	8537.0	8.5370E5	3.383E-3	0.4	2.4	143.992	690.81	300.0
222.8	375.0	0.5942	23.996	22.4	186.0	7204.8999	10000	0.04565	1.323E-3	9006.1	9.0061E5	3.383E-3	0.4	2.4	144.996	683.60	300.0
225.3	375.0	0.6009	24.996	22.4	176.1	7456.2002	10000	0.04322	1.252E-3	9320.3	9.3203E5	3.384E-3	0.4	2.4	145.996	691.26	300.0
224.6	375.0	0.5990	25.992	22.4	195.9	7707.5498	10000	0.04809	1.393E-3	9634.4	9.6344E5	3.384E-3	0.4	2.4	146.992	689.14	300.0
227.7	375.0	0.6071	26.992	22.4	165.3	8084.7100	10000	0.04058	1.176E-3	10106	1.0106E6	3.384E-3	0.4	2.5	147.992	698.48	300.0
226.3	375.0	0.6034	27.992	22.4	169.5	8337.3896	10000	0.04159	1.205E-3	10422	1.0422E6	3.384E-3	0.5	2.5	148.992	694.18	300.0
225.7	375.0	0.6020	29.000	22.4	160.4	8712.8203	10000	0.03936	1.140E-3	10891	1.0891E6	3.384E-3	0.5	2.5	150.000	692.53	300.0
223.7	375.0	0.5965	29.992	22.4	178.6	8964.5596	10000	0.04382	1.270E-3	11206	1.1206E6	3.384E-3	0.5	2.5	150.992	686.33	300.0

Continuous ramp step 2

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

219.5	372.3	0.5896	1.0040	22.4	186.8	211.9820	10000	0.04585	1.348E-3	264.98	26498	3.384E-3	0.0	2.5	152.004	673.56	297.9
215.4	364.8	0.5906	2.0120	22.4	178.6	568.8780	10000	0.04382	1.342E-3	711.10	71110	3.383E-3	0.0	2.6	153.012	660.97	291.8
212.4	359.7	0.5906	3.0200	22.4	213.3	806.9750	10000	0.05235	1.649E-3	1008.7	1.0087E5	3.383E-3	0.1	2.6	154.020	651.74	287.7
205.2	352.0	0.5831	4.0040	22.4	191.0	1157.6500	10000	0.04687	1.541E-3	1447.1	1.4471E5	3.384E-3	0.1	2.6	155.004	629.66	281.6
198.5	347.0	0.5721	5.0200	22.4	195.9	1383.1300	10000	0.04809	1.627E-3	1728.9	1.7289E5	3.384E-3	0.1	2.6	156.020	609.05	277.6
190.5	339.4	0.5612	6.0080	22.4	262.9	1721.2300	10000	0.06452	2.282E-3	2151.5	2.1515E5	3.384E-3	0.1	2.6	157.008	584.36	271.5
186.7	334.2	0.5585	7.0120	22.4	233.9	1946.5300	10000	0.05742	2.094E-3	2433.2	2.4332E5	3.384E-3	0.1	2.6	158.012	572.65	267.4
182.3	326.7	0.5582	8.0200	22.4	200.0	2267.0100	10000	0.04910	1.875E-3	2833.8	2.8338E5	3.384E-3	0.1	2.7	159.020	559.44	261.3
174.8	321.6	0.5435	9.0200	22.4	245.5	2478.7200	10000	0.06026	2.374E-3	3098.4	3.0984E5	3.384E-3	0.2	2.7	160.020	536.20	257.3
170.5	316.4	0.5387	10.024	22.4	233.1	2691.3999	10000	0.05722	2.328E-3	3364.3	3.3643E5	3.384E-3	0.2	2.7	161.024	523.00	253.1
162.0	308.8	0.5247	11.020	22.4	253.8	2998.2900	10000	0.06229	2.662E-3	3747.9	3.7479E5	3.384E-3	0.2	2.7	162.020	497.05	247.0
158.7	303.7	0.5226	12.020	22.4	245.5	3198.3401	10000	0.06026	2.662E-3	3997.9	3.9979E5	3.384E-3	0.2	2.7	163.020	486.92	243.0
151.5	295.9	0.5120	13.020	22.4	284.4	3498.7900	10000	0.06979	3.247E-3	4373.5	4.3735E5	3.384E-3	0.2	2.7	164.020	464.92	236.8
145.9	290.8	0.5020	14.020	22.4	301.7	3692.7400	10000	0.07406	3.569E-3	4615.9	4.6159E5	3.384E-3	0.2	2.8	165.020	447.76	232.6
145.6	285.7	0.5096	15.020	22.4	267.0	3880.8000	10000	0.06553	3.271E-3	4851.0	4.8510E5	3.383E-3	0.3	2.8	166.020	446.67	228.6
138.4	278.0	0.4977	16.008	22.4	285.2	4162.8398	10000	0.07000	3.690E-3	5203.6	5.2036E5	3.383E-3	0.3	2.8	167.008	424.47	222.4
132.7	272.8	0.4863	17.020	22.4	281.1	4343.4902	10000	0.06898	3.777E-3	5429.4	5.4294E5	3.384E-3	0.3	2.8	168.020	407.01	218.2
128.6	265.2	0.4849	18.000	22.4	281.1	4606.2500	10000	0.06898	3.995E-3	5757.8	5.7578E5	3.383E-3	0.3	2.8	169.000	394.57	212.2
123.5	260.1	0.4750	19.020	22.4	293.5	4781.2002	10000	0.07203	4.338E-3	5976.5	5.9765E5	3.383E-3	0.3	2.8	170.020	379.04	208.1
119.6	254.8	0.4694	20.004	22.4	301.7	4956.3701	10000	0.07406	4.646E-3	6195.5	6.1955E5	3.384E-3	0.3	2.9	171.004	366.95	203.9
113.2	247.2	0.4580	21.020	22.4	305.9	5201.5298	10000	0.07507	5.004E-3	6501.9	6.5019E5	3.383E-3	0.4	2.9	172.020	347.39	197.8
109.3	242.1	0.4516	22.020	22.4	306.7	5362.7402	10000	0.07527	5.234E-3	6703.4	6.7034E5	3.383E-3	0.4	2.9	173.020	335.40	193.7
104.6	234.3	0.4464	23.020	22.4	323.2	5604.6602	10000	0.07933	5.890E-3	7005.8	7.0058E5	3.383E-3	0.4	2.9	174.020	320.82	187.4
99.95	229.3	0.4360	24.076	22.4	312.5	5750.3799	10000	0.07669	5.945E-3	7188.0	7.1880E5	3.383E-3	0.4	2.9	175.076	306.63	183.4
92.34	221.5	0.4168	25.020	22.4	344.7	5976.2100	10000	0.08461	7.024E-3	7470.3	7.4703E5	3.383E-3	0.4	2.9	176.020	283.29	177.2
88.93	216.2	0.4113	26.020	22.4	343.1	6125.2500	10000	0.08420	7.337E-3	7656.6	7.6566E5	3.384E-3	0.4	3.0	177.020	272.82	173.0
87.39	211.1	0.4139	27.020	22.4	320.7	6262.6602	10000	0.07872	7.195E-3	7828.3	7.8283E5	3.384E-3	0.5	3.0	178.020	268.12	168.9
80.90	203.5	0.3976	28.008	22.4	343.9	6471.5698	10000	0.08440	8.308E-3	8089.5	8.0895E5	3.384E-3	0.5	3.0	179.008	248.19	162.8
78.77	198.2	0.3975	29.004	22.4	348.0	6606.2598	10000	0.08542	8.863E-3	8257.8	8.2578E5	3.384E-3	0.5	3.0	180.004	241.66	158.5
75.15	192.8	0.3897	30.020	22.4	343.9	6801.6299	10000	0.08440	9.247E-3	8502.0	8.5020E5	3.384E-3	0.5	3.0	181.020	230.55	154.3
69.26	185.2	0.3740	31.004	22.4	355.5	6927.9102	10000	0.08724	0.01037	8659.9	8.6599E5	3.384E-3	0.5	3.0	182.004	212.49	148.1
66.27	179.9	0.3684	32.008	22.4	371.2	7050.5098	10000	0.09110	0.01147	8813.1	8.8131E5	3.384E-3	0.5	3.1	183.008	203.31	143.9
62.36	172.1	0.3624	33.020	22.4	371.2	7224.2598	10000	0.09110	0.01254	9030.3	9.0303E5	3.384E-3	0.6	3.1	184.020	191.33	137.6
59.27	166.9	0.3550	34.024	22.4	360.4	7336.5801	10000	0.08846	0.01293	9170.7	9.1707E5	3.384E-3	0.6	3.1	185.024	181.83	133.6
55.39	161.7	0.3426	35.108	22.4	384.4	7448.7202	10000	0.09434	0.01471	9310.9	9.3109E5	3.384E-3	0.6	3.1	186.108	169.94	129.3
51.42	153.5	0.3349	36.020	22.4	384.4	7610.8799	10000	0.09434	0.01630	9513.6	9.5136E5	3.384E-3	0.6	3.1	187.020	157.75	122.8
49.04	148.4	0.3304	37.020	22.4	384.4	7710.5801	10000	0.09434	0.01745	9638.2	9.6382E5	3.384E-3	0.6	3.1	188.020	150.44	118.7
46.47	143.1	0.3247	38.004	22.4	386.0	7810.7798	10000	0.09475	0.01884	9763.5	9.7635E5	3.384E-3	0.6	3.2	189.004	142.58	114.5
41.73	135.0	0.3091	39.024	22.4	389.4	7953.8501	10000	0.09556	0.02136	9942.3	9.9423E5	3.384E-3	0.7	3.2	190.024	128.02	108.0
38.92	129.9	0.2995	40.024	22.4	396.0	8043.9199	10000	0.09718	0.02346	10055	1.0055E6	3.384E-3	0.7	3.2	191.024	119.40	103.9
36.33	124.6	0.2915	41.020	22.4	398.4	8127.7100	10000	0.09779	0.02566	10160	1.0160E6	3.383E-3	0.7	3.2	192.020	111.46	99.69
32.20	116.4	0.2765	42.016	22.4	409.2	8252.0703	10000	0.1004	0.03018	10315	1.0315E6	3.384E-3	0.7	3.2	193.016	98.784	93.15
30.35	111.4	0.2725	43.008	22.4	388.5	8326.6299	10000	0.09536	0.03133	10408	1.0408E6	3.383E-3	0.7	3.2	194.008	93.115	89.09
28.28	106.1	0.2667	44.004	22.4	400.1	8401.5098	10000	0.09820	0.03557	10502	1.0502E6	3.383E-3	0.7	3.3	195.004	86.772	84.85
25.81	100.5	0.2568	45.004	22.4	406.7	8475.5303	10000	0.09982	0.04028	10594	1.0594E6	3.383E-3	0.8	3.3	196.004	79.180	80.39
22.64	92.27	0.2454	46.004	22.4	414.2	8574.7803	10000	0.1016	0.04864	10718	1.0718E6	3.383E-3	0.8	3.3	197.004	69.466	73.82
20.52	86.92	0.2360	47.016	22.4	406.7	8639.2695	10000	0.09982	0.05383	10799	1.0799E6	3.383E-3	0.8	3.3	198.016	62.942	69.54
18.14	81.22	0.2233	48.020	22.4	410.8	8699.1104	10000	0.1008	0.06228	10874	1.0874E6	3.383E-3	0.8	3.3	199.020	55.646	64.98
16.00	75.43	0.2121	49.020	22.4	413.3	8754.1602	10000	0.1014	0.07265	10943	1.0943E6	3.383E-3	0.8	3.3	200.020	49.084	60.34
13.18	67.40	0.1955	50.020	22.4	429.9	8828.2002	10000	0.1055	0.09463	11035	1.1035E6	3.383E-3	0.8	3.4	201.020	40.429	53.92
11.39	61.49	0.1852	51.008	22.4	422.4	8877.3203	10000	0.1037	0.1117	11097	1.1097E6	3.384E-3	0.9	3.4	202.008	34.935	49.19
9.727	55.40	0.1756	52.020	22.4	421.6	8920.2695	10000	0.1035	0.1373	11150	1.1150E6	3.384E-3	0.9	3.4	203.020	29.841	44.32
8.104	49.99	0.1621	53.004	22.4	430.7	8957.0000	10000	0.1057	0.1723	11196	1.1196E6	3.383E-3	0.9	3.4	204.004	24.864	40.00
6.402	43.97	0.1456	54.020	22.4	430.7	8993.4902	10000	0.1057	0.2228	11242	1.1242E6	3.384E-3	0.9	3.4	205.020	19.641	35.17
4.972	37.66	0.1320	55.020	22.4	423.2	9023.9404	10000	0.1039	0.2984	11280	1.1280E6	3.383E-3	0.9	3.4	206.020	15.255	30.13
3.754	32.29	0.1163	56.020	22.4	443.9	9047.9404	10000	0.1090	0.4258	11310	1.1310E6	3.383E-3	0.9	3.5	207.020	11.516	25.83
2.612	25.92	0.1008	57.008	22.4	453.8	9071.9199	10000	0.1114	0.6756	11340	1.1340E6	3.383E-3	1.0	3.5	208.008	8.0133	20.73
1.961	22.13	0.08862	58.004	22.4	440.6	9083.2500	10000	0.1081	0.8998	11354	1.1354E6	3.383E-3	1.0	3.5	209.004	6.0167	17.70
0.8815	13.65	0.06459	59.020	22.4	439.8	9099.9502	10000	0.1079	2.361	11375	1.1375E6	3.384E-3	1.0	3.5	210.020	2.7045	10.92
0.2105	6.434	0.03272	60.020	22.4	436.5	9107.7402	10000	0.1071	10.54	11385	1.1385E6	3.384E-3	1.0	3.5	211.020	0.64578	5.147

